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Abstract— Isomerization during grinding of solid‐state α‐monohydrate, α‐anhydrate and β‐anhydrate of lactose was investigated. Samples were ground in an agate centrifugal ball‐mill at 270 rev min −1 at room temperature (20C). The crystallinity of ground lactose was measured by Hermans' method from the powder X‐ray diffraction profiles.
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